1,6,13,18,25,30-hexaoxa[6.6.6](1,3,5)cyclophane. attempted synthesis of a [4] cryptand

W. David Curtis, J. Fraser Stoddart*, Graham H. Jones

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

8 Scopus citations

Abstract

The hexaoxa[5.5.5] (1.3.5)cyclophane (12) has been synthesised from phloroglucinol and 1.4-dibromobutane by using a stepwise approach. All attempts to effect catalytic hydrogenation of both aromatic rings in the hexaoxa- [6.6.6] (1.3.5)cyclophane (12) to give the desired [4]cryptand (14) have proved unsuccessful.

Original languageEnglish (US)
Pages (from-to)785-788
Number of pages4
JournalJournal of the Chemical Society, Perkin Transactions 1
DOIs
StatePublished - 1977

ASJC Scopus subject areas

  • Chemistry(all)

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