1,6,13,18,25,30-hexaoxa[6.6.6](1,3,5)cyclophane. attempted synthesis of a [4] cryptand

W. David Curtis; J. Fraser Stoddart; Graham H. Jones

doi:10.1039/P19770000785

1,6,13,18,25,30-hexaoxa[6.6.6](1,3,5)cyclophane. attempted synthesis of a [4] cryptand

W. David Curtis, J. Fraser Stoddart^*, Graham H. Jones

^*Corresponding author for this work

Chemistry

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

The hexaoxa[5.5.5] (1.3.5)cyclophane (12) has been synthesised from phloroglucinol and 1.4-dibromobutane by using a stepwise approach. All attempts to effect catalytic hydrogenation of both aromatic rings in the hexaoxa- [6.6.6] (1.3.5)cyclophane (12) to give the desired [4]cryptand (14) have proved unsuccessful.

Original language	English (US)
Pages (from-to)	785-788
Number of pages	4
Journal	Journal of the Chemical Society, Perkin Transactions 1
DOIs	https://doi.org/10.1039/P19770000785
State	Published - 1977

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Chemistry(all)

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abstract = "The hexaoxa[5.5.5] (1.3.5)cyclophane (12) has been synthesised from phloroglucinol and 1.4-dibromobutane by using a stepwise approach. All attempts to effect catalytic hydrogenation of both aromatic rings in the hexaoxa- [6.6.6] (1.3.5)cyclophane (12) to give the desired [4]cryptand (14) have proved unsuccessful.",

author = "{David Curtis}, W. and Stoddart, {J. Fraser} and Jones, {Graham H.}",

year = "1977",

doi = "10.1039/P19770000785",

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pages = "785--788",

journal = "Journal of the Chemical Society, Perkin Transactions 1",

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T1 - 1,6,13,18,25,30-hexaoxa[6.6.6](1,3,5)cyclophane. attempted synthesis of a [4] cryptand

AU - David Curtis, W.

AU - Stoddart, J. Fraser

AU - Jones, Graham H.

PY - 1977

Y1 - 1977

N2 - The hexaoxa[5.5.5] (1.3.5)cyclophane (12) has been synthesised from phloroglucinol and 1.4-dibromobutane by using a stepwise approach. All attempts to effect catalytic hydrogenation of both aromatic rings in the hexaoxa- [6.6.6] (1.3.5)cyclophane (12) to give the desired [4]cryptand (14) have proved unsuccessful.

AB - The hexaoxa[5.5.5] (1.3.5)cyclophane (12) has been synthesised from phloroglucinol and 1.4-dibromobutane by using a stepwise approach. All attempts to effect catalytic hydrogenation of both aromatic rings in the hexaoxa- [6.6.6] (1.3.5)cyclophane (12) to give the desired [4]cryptand (14) have proved unsuccessful.

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ER -

1,6,13,18,25,30-hexaoxa[6.6.6](1,3,5)cyclophane. attempted synthesis of a [4] cryptand

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