2-(1,3-Dithian-2-yl)benzaldehyde and N-{2-[2-(1,3-dioxan-2-yl)phenoxy]ethyl}phthalimide

Paul G. Jene; James A. Ibers

doi:10.1107/S010827010000353X

2-(1,3-Dithian-2-yl)benzaldehyde and N-{2-[2-(1,3-dioxan-2-yl)phenoxy]ethyl}phthalimide

Paul G. Jene, James A. Ibers

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

The crystal structures of two elaborated-porphyrin precursors have been determined. In the crystalline state, 2-(1,3-dithian-2-yl)benzaldehyde, C₁₁H₁₂OS₂, has its dithiane ring in a slightly distorted chair conformation. The molecules pack in anti-parallel chains. N-{2-[2-(1,3-Dioxan-2-yl)phenoxy]ethyl}-phthalimide, C₂₀H₁₉NO₅, is in a folded conformation. The dihedral angle between the phthalimide and phenyl planes is 80.07 (3)°. In the crystalline states, molecules stack on top of one another.

Original language	English (US)
Pages (from-to)	705-707
Number of pages	3
Journal	Acta Crystallographica, Section C: Crystal Structure Communications
Volume	56
Issue number	6
DOIs	https://doi.org/10.1107/S010827010000353X
State	Published - Jun 2000
Externally published	Yes

ASJC Scopus subject areas

Biochemistry, Genetics and Molecular Biology(all)

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10.1107/S010827010000353X

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title = "2-(1,3-Dithian-2-yl)benzaldehyde and N-{2-[2-(1,3-dioxan-2-yl)phenoxy]ethyl}phthalimide",

abstract = "The crystal structures of two elaborated-porphyrin precursors have been determined. In the crystalline state, 2-(1,3-dithian-2-yl)benzaldehyde, C11H12OS2, has its dithiane ring in a slightly distorted chair conformation. The molecules pack in anti-parallel chains. N-{2-[2-(1,3-Dioxan-2-yl)phenoxy]ethyl}-phthalimide, C20H19NO5, is in a folded conformation. The dihedral angle between the phthalimide and phenyl planes is 80.07 (3)°. In the crystalline states, molecules stack on top of one another.",

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year = "2000",

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doi = "10.1107/S010827010000353X",

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T1 - 2-(1,3-Dithian-2-yl)benzaldehyde and N-{2-[2-(1,3-dioxan-2-yl)phenoxy]ethyl}phthalimide

AU - Jene, Paul G.

AU - Ibers, James A.

PY - 2000/6

Y1 - 2000/6

N2 - The crystal structures of two elaborated-porphyrin precursors have been determined. In the crystalline state, 2-(1,3-dithian-2-yl)benzaldehyde, C11H12OS2, has its dithiane ring in a slightly distorted chair conformation. The molecules pack in anti-parallel chains. N-{2-[2-(1,3-Dioxan-2-yl)phenoxy]ethyl}-phthalimide, C20H19NO5, is in a folded conformation. The dihedral angle between the phthalimide and phenyl planes is 80.07 (3)°. In the crystalline states, molecules stack on top of one another.

AB - The crystal structures of two elaborated-porphyrin precursors have been determined. In the crystalline state, 2-(1,3-dithian-2-yl)benzaldehyde, C11H12OS2, has its dithiane ring in a slightly distorted chair conformation. The molecules pack in anti-parallel chains. N-{2-[2-(1,3-Dioxan-2-yl)phenoxy]ethyl}-phthalimide, C20H19NO5, is in a folded conformation. The dihedral angle between the phthalimide and phenyl planes is 80.07 (3)°. In the crystalline states, molecules stack on top of one another.

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JO - Acta Crystallographica Section C: Crystal Structure Communications

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2-(1,3-Dithian-2-yl)benzaldehyde and N-{2-[2-(1,3-dioxan-2-yl)phenoxy]ethyl}phthalimide

Abstract

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CCDC 146064: Experimental Crystal Structure Determination

CCDC 146065: Experimental Crystal Structure Determination

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2-(1,3-Dithian-2-yl)benzaldehyde and N-{2-[2-(1,3-dioxan-2-yl)phenoxy]ethyl}phthalimide

Abstract

ASJC Scopus subject areas

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Datasets

CCDC 146064: Experimental Crystal Structure Determination

CCDC 146065: Experimental Crystal Structure Determination

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