TY - JOUR
T1 - Cryo diffraction microscopy
T2 - Ice conditions and finite supports
AU - Miao, H.
AU - Downing, K.
AU - Huang, X.
AU - Kirz, J.
AU - Marchesini, S.
AU - Nelson, J.
AU - Shapiro, D.
AU - Steinbrener, J.
AU - Stewart, A.
AU - Jacobsen, C.
PY - 2009
Y1 - 2009
N2 - Cryo specimen conditions greatly alleviate radiation damage in x-ray microscopy. In diffraction microscopy with plane-wave illumination, a finite support constraint is required in order to obtain a reconstructed image, but this demands that there be an area outside the specimen which is free of optical response. We report here observations based on our early attempts in cryo diffraction microscopy, where ice scatter from outside the cell and ice deposition during data taking have been problems. We outline solutions that are being implemented for future experiments.
AB - Cryo specimen conditions greatly alleviate radiation damage in x-ray microscopy. In diffraction microscopy with plane-wave illumination, a finite support constraint is required in order to obtain a reconstructed image, but this demands that there be an area outside the specimen which is free of optical response. We report here observations based on our early attempts in cryo diffraction microscopy, where ice scatter from outside the cell and ice deposition during data taking have been problems. We outline solutions that are being implemented for future experiments.
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U2 - 10.1088/1742-6596/186/1/012055
DO - 10.1088/1742-6596/186/1/012055
M3 - Article
AN - SCOPUS:73649148731
SN - 1742-6588
VL - 186
JO - Journal of Physics: Conference Series
JF - Journal of Physics: Conference Series
M1 - 012055
ER -