Abstract
The temporal evolution of the nanostructure and chemistry of a model Ni-8.5 at.% Cr-10 at.% Al alloy, with the addition of 2 at.% Re, aged at 1073 K from 0.25 to 264 h, was studied. Transmission electron microscopy and atom-probe tomography were used to measure the number density and mean radius of the γ′ (L12 structure)-precipitates and the chemistry of the γ′-precipitates and the γ (face-centered cubic)-matrix, including the partitioning behavior of all alloying elements between the γ- and γ′-phases and the segregation behavior at γ/γ′ interfaces. The precipitates remained spheroidal for an aging time of up to 264 h and, unlike commercial nickel-based superalloys containing Re, there was not confined (nonmonotonic) Re segregation at the γ/γ′ interfaces.
Original language | English (US) |
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Pages (from-to) | 1145-1157 |
Number of pages | 13 |
Journal | Acta Materialia |
Volume | 55 |
Issue number | 4 |
DOIs | |
State | Published - Feb 2007 |
Funding
The National Science Foundation, Division of Materials Research sponsored this research under grant DMR-0241928. K. E. Yoon received partial support from a National Aeronautics and Space Administration Graduate Student Researcher Program fellowship. Special thanks to A. Panzanella (National Aeronautics and Space Administration Glenn Center) for electro-discharge machining all the APT sample blanks and to Drs. A. Umantsev and C. K. Sudbrack for reading the manuscript.
Keywords
- Atom probe tomography
- Nanostructure
- Nickel alloys
- Rhenium
- Segregation
ASJC Scopus subject areas
- Electronic, Optical and Magnetic Materials
- Ceramics and Composites
- Polymers and Plastics
- Metals and Alloys