Fabrication of a novel chromium-iron oxide (Cr2Fe6O12) nanoparticles by thermal treatment method

Mahmoud Goodarz Naseri; Halimah Mohamed Kamari; Arash Dehzangi; Ahmad Kamalianfar; Elias B. Saion

doi:10.1016/j.jmmm.2015.04.013

Fabrication of a novel chromium-iron oxide (Cr₂Fe₆O₁₂) nanoparticles by thermal treatment method

Mahmoud Goodarz Naseri^*, Halimah Mohamed Kamari, Arash Dehzangi, Ahmad Kamalianfar, Elias B. Saion

^*Corresponding author for this work

Center for Quantum Devices (CQD)

Research output: Contribution to journal › Article › peer-review

20 Scopus citations

Abstract

In this research,a novel chromium-iron oxide (Cr₂Fe₆O₁₂) nanoparticle with rhombohedral symmetry was prepared by a simple thermal treatment method.Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 773 and 923 K, where the produced chromium-ironoxide nanoparticles had different crystallite sizes ranging from 9 to 20 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). The samples demonstrated a magnetic behavior with unpaired electron spins, which was confirmed by using vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy.

Original language	English (US)
Pages (from-to)	113-119
Number of pages	7
Journal	Journal of Magnetism and Magnetic Materials
Volume	389
DOIs	https://doi.org/10.1016/j.jmmm.2015.04.013
State	Published - Sep 1 2015

Funding

This work was supported by the Ministry of Higher Education of Malaysia under the FRGS grant , Universiti Putra Malaysia under the RUGS grant and Malayer University of Iran .

Keywords

Calcination X-ray diffraction Magnetic properties Electron paramagnetic resonance

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Condensed Matter Physics

Access to Document

10.1016/j.jmmm.2015.04.013

Cite this

@article{f679b3ceae904d5190741ee8decd67a5,

title = "Fabrication of a novel chromium-iron oxide (Cr2Fe6O12) nanoparticles by thermal treatment method",

abstract = "In this research,a novel chromium-iron oxide (Cr2Fe6O12) nanoparticle with rhombohedral symmetry was prepared by a simple thermal treatment method.Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 773 and 923 K, where the produced chromium-ironoxide nanoparticles had different crystallite sizes ranging from 9 to 20 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). The samples demonstrated a magnetic behavior with unpaired electron spins, which was confirmed by using vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy.",

keywords = "Calcination X-ray diffraction Magnetic properties Electron paramagnetic resonance",

author = "Naseri, {Mahmoud Goodarz} and Kamari, {Halimah Mohamed} and Arash Dehzangi and Ahmad Kamalianfar and Saion, {Elias B.}",

note = "Publisher Copyright: {\textcopyright} 2015 Published by Elsevier B.V.",

year = "2015",

month = sep,

day = "1",

doi = "10.1016/j.jmmm.2015.04.013",

language = "English (US)",

volume = "389",

pages = "113--119",

journal = "Journal of Magnetism and Magnetic Materials",

issn = "0304-8853",

publisher = "Elsevier B.V.",

}

TY - JOUR

T1 - Fabrication of a novel chromium-iron oxide (Cr2Fe6O12) nanoparticles by thermal treatment method

AU - Naseri, Mahmoud Goodarz

AU - Kamari, Halimah Mohamed

AU - Dehzangi, Arash

AU - Kamalianfar, Ahmad

AU - Saion, Elias B.

PY - 2015/9/1

Y1 - 2015/9/1

N2 - In this research,a novel chromium-iron oxide (Cr2Fe6O12) nanoparticle with rhombohedral symmetry was prepared by a simple thermal treatment method.Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 773 and 923 K, where the produced chromium-ironoxide nanoparticles had different crystallite sizes ranging from 9 to 20 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). The samples demonstrated a magnetic behavior with unpaired electron spins, which was confirmed by using vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy.

AB - In this research,a novel chromium-iron oxide (Cr2Fe6O12) nanoparticle with rhombohedral symmetry was prepared by a simple thermal treatment method.Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 773 and 923 K, where the produced chromium-ironoxide nanoparticles had different crystallite sizes ranging from 9 to 20 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). The samples demonstrated a magnetic behavior with unpaired electron spins, which was confirmed by using vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy.

KW - Calcination X-ray diffraction Magnetic properties Electron paramagnetic resonance

UR - http://www.scopus.com/inward/record.url?scp=84928254450&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84928254450&partnerID=8YFLogxK

U2 - 10.1016/j.jmmm.2015.04.013

DO - 10.1016/j.jmmm.2015.04.013

M3 - Article

AN - SCOPUS:84928254450

SN - 0304-8853

VL - 389

SP - 113

EP - 119

JO - Journal of Magnetism and Magnetic Materials

JF - Journal of Magnetism and Magnetic Materials

ER -