Fracture toughness and impact damage resistance of nanoreinforced Carbon/Epoxy composites

Joel S. Fenner, Isaac M Daniel*

*Corresponding author for this work

Research output: Contribution to journalConference article

Abstract

In this study, the objective was to develop, manufacture, and test hybrid nano/microcomposites with a nanoparticle reinforced matrix and demonstrate improvements to damage tolerance via Mode-II fracture toughness and impact damage absorption. The material employed was a woven carbon fiber/epoxy composite, with multi-wall carbon nanotubes as a nano-scale reinforcement to the matrix. A direct-mixing process, aided by a block copolymer dispersant and sonication, was employed to produce the nanoparticle-filled epoxy matrix. Fracture toughness was tested by several different Mode- II and mixed Mode-I/Mode-II specimens to determine the toughness improvement. Testing and material difficulties were overcome by this approach, showing a Mode-II toughness improvement of approx. 35% in the hybrid material. Impact tests were performed in a falling-weight drop tower at different energies to introduce interlaminar damage in samples of both materials. Impact damaged specimens were imaged by ultrasonic c-scans to assess the area of the damage zone at each ply interface. Post-mortem optical microscopy confirmed the interlaminar nature of the impact damage. These tests showed a consistently smaller absorbed energy and smaller total damage area for hybrid composite over reference material, translating to a nominally higher ‘effective impact toughness’ in the hybrid composite (approx 42%) regardless of specific impact energy.

Original languageEnglish (US)
Pages (from-to)213-224
Number of pages12
JournalConference Proceedings of the Society for Experimental Mechanics Series
Volume8
Issue number2016
DOIs
StatePublished - Jan 1 2016
Event2015 SEM Annual Conference and Exposition on Experimental and Applied Mechanics - Costa Mesa, United States
Duration: Jun 8 2015Jun 11 2015

Fingerprint

Fracture toughness
Carbon
Composite materials
Toughness
Nanoparticles
Damage tolerance
Sonication
Hybrid materials
Towers
Block copolymers
Carbon fibers
Optical microscopy
Carbon nanotubes
Reinforcement
Ultrasonics
Testing

Keywords

  • Fracture toughness
  • Hybrid nano/microcomposites
  • Impact behavior
  • Nanocomposites
  • Test methods

ASJC Scopus subject areas

  • Engineering(all)
  • Computational Mechanics
  • Mechanical Engineering

Cite this

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title = "Fracture toughness and impact damage resistance of nanoreinforced Carbon/Epoxy composites",
abstract = "In this study, the objective was to develop, manufacture, and test hybrid nano/microcomposites with a nanoparticle reinforced matrix and demonstrate improvements to damage tolerance via Mode-II fracture toughness and impact damage absorption. The material employed was a woven carbon fiber/epoxy composite, with multi-wall carbon nanotubes as a nano-scale reinforcement to the matrix. A direct-mixing process, aided by a block copolymer dispersant and sonication, was employed to produce the nanoparticle-filled epoxy matrix. Fracture toughness was tested by several different Mode- II and mixed Mode-I/Mode-II specimens to determine the toughness improvement. Testing and material difficulties were overcome by this approach, showing a Mode-II toughness improvement of approx. 35{\%} in the hybrid material. Impact tests were performed in a falling-weight drop tower at different energies to introduce interlaminar damage in samples of both materials. Impact damaged specimens were imaged by ultrasonic c-scans to assess the area of the damage zone at each ply interface. Post-mortem optical microscopy confirmed the interlaminar nature of the impact damage. These tests showed a consistently smaller absorbed energy and smaller total damage area for hybrid composite over reference material, translating to a nominally higher ‘effective impact toughness’ in the hybrid composite (approx 42{\%}) regardless of specific impact energy.",
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Fracture toughness and impact damage resistance of nanoreinforced Carbon/Epoxy composites. / Fenner, Joel S.; Daniel, Isaac M.

In: Conference Proceedings of the Society for Experimental Mechanics Series, Vol. 8, No. 2016, 01.01.2016, p. 213-224.

Research output: Contribution to journalConference article

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