Hierarchical and operando tomography with x-rays and beyond

Christoph Rau*, Darren Batey, Shashi Marathe, Leonard Turpin, Kudakwashe Jakata, Silvia Cipiccia, Isabel Antony, Roberto Volpe, Claus Peter Richter, Alessandra Carriero, Maud Dumoux, Jürgen E. Schneider, Erica Dall’Armellina, Marc W. Holderied, Jan Van den Bulcke

*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceedingConference contribution

1 Scopus citations

Abstract

We report about the experimental work related to hierarchical structures at the Diamond I13L beamlines. The I13-2 Imaging and I13-1 Coherence beamlines provide imaging with micro- and nano-resolution. The Diamond II upgrade for the synchrotron source and the OCTOPI upgrade for I13L provide new opportunities for expanding the existing scientific areas in multiscale and operando imaging. We describe the scientific research benefitting from the instrumental upgrade. Comparable recording times across all length scales will enable hierarchical operando imaging. With the implementation of automated high-throughput data acquisition and analysis, large numbers of samples will be analyzed.

Original languageEnglish (US)
Title of host publicationDevelopments in X-Ray Tomography XV
EditorsBert Muller, Ge Wang
PublisherSPIE
ISBN (Electronic)9781510679641
DOIs
StatePublished - 2024
Event15th SPIE Conference on Developments in X-Ray Tomography - San Diego, United States
Duration: Aug 19 2024Aug 22 2024

Publication series

NameProceedings of SPIE - The International Society for Optical Engineering
Volume13152
ISSN (Print)0277-786X
ISSN (Electronic)1996-756X

Conference

Conference15th SPIE Conference on Developments in X-Ray Tomography
Country/TerritoryUnited States
CitySan Diego
Period8/19/248/22/24

Funding

Kaz Wanelik, Huw Shorthouse, Tim Ardern and all support teams at Diamond Light Source are greatly acknowledged for their work at the beamlines. Sylvia Britto and Konstantin Ignatyev from I18 provided help with their furnace for the pyrolysis experiments. The work is supported by the Diamond-Manchester collaboration. The contributions to the experiments by the different research teams, namely Luis Salinas-Farran, Maryanne Mosonik, (R. Volpe, Queen Mary, London), G. Broad, B. Price, O. Kippax-Chui (A. Goswami, NHM, London), Asier Munoz, Maialen Ugarteburu (A. Carriero CCNY, New York), M. Farzi, I. Teh (J. Schneider, Leeds), Louis Verschuren, Sofie Dierickx, Matthieu Boone (J. Van den Bulcke, UGCT-UGent), are greatly appreciated. The present publication is dedicated to Ljubo Zaja, who contributed substantially to the engineering work at the beamline and lately to the automated sample changer project.

Keywords

  • High-Throughput
  • Multiscale
  • Operando
  • Synchrotron
  • Tomography

ASJC Scopus subject areas

  • Electronic, Optical and Magnetic Materials
  • Condensed Matter Physics
  • Computer Science Applications
  • Applied Mathematics
  • Electrical and Electronic Engineering

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