Plasma cleaning and its applications for electron microscopy

Thomas C. Isabell*, Paul E. Fischione, Catherine O'Keefe, Murat U. Guruz, Vinayak P. Dravid

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

64 Scopus citations

Abstract

The effectiveness of applying a high-frequency, low-energy, reactive gas plasma for the removal of hydrocarbon contamination from specimens and components for electron microscopy has been investigated with a variety of analytical techniques. Transmission electron microscopy (TEM) analysis of specimens that have been plasma cleaned shows an elimination of the carbonaceous contamination from the specimen. With extended cleaning times the removal of existing carbon contamination debris due to previously conducted microanalysis is shown. Following plasma cleaning, specimens may be examined in the electron microscope for several hours without exhibiting evidence of recontamination. The effectiveness of plasma cleaning is not limited to applications for TEM specimens. Scanning electron microscopy (SEM) specimens that have been plasma cleaned likewise show an elimination of carbonaceous contamination. Furthermore, other electron microscopy parts and accessories, such as aperture strips, specimen clamping rings, and Wehnelts, among others, can benefit from plasma cleaning.

Original languageEnglish (US)
Pages (from-to)126-135
Number of pages10
JournalMicroscopy and Microanalysis
Volume5
Issue number2
DOIs
StatePublished - 1999

Keywords

  • Electron energy-loss spectrometry (EELS)
  • Energy dispersive X-ray spectrometry (EDS)
  • Inductive plasma
  • Plasma cleaning
  • Specimen preparation

ASJC Scopus subject areas

  • Instrumentation

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