Abstract
In situ synchrotron X-ray diffraction measurements are used to create two-dimensional maps of elastic strain and texture, averaged over a compact-tension specimen thickness, near a crack tip in a martensitic NiTi alloy. After fatigue crack propagation, the material ahead of the crack and in its wake exhibits a strong texture, which is eliminated by subsequent shape-memory heat treatment, indicating that this texture is due to detwinning, the main deformation mechanism of NiTi. Upon subsequent application of a static tensile stresses, the highly textured zone reappears and grows around the crack tip as the applied stress is increased. At the highest applied stress intensity of 35 MPa m1/2, large tensile strains are measured ahead of the crack tip and considerable elastic anisotropy is observed. This detwinning zone is similar to the plastic zone produced by dislocation slip present around cracks in other metals. The texture in this zone is not significantly altered after mechanical unloading, despite the development of substantial triaxial compressive residual strains in this zone.
Original language | English (US) |
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Pages (from-to) | 3929-3942 |
Number of pages | 14 |
Journal | Acta Materialia |
Volume | 55 |
Issue number | 11 |
DOIs | |
State | Published - Jun 2007 |
Funding
Use of the Advanced Photon Source was supported by the US Department of Energy, Office of Science, Office of Basic Energy Sciences, under Contract No. DE-AC02-06CH11357 is supported by the Natural Sciences and Engineering Research Council of Canada. D.C.D. acknowledges support from the US National Science Foundation through Grant DMR-0505772/001.
Keywords
- Ni-Ti
- Nitinol
- Shape memory
- Smart materials
- Superelasticity
ASJC Scopus subject areas
- Electronic, Optical and Magnetic Materials
- Ceramics and Composites
- Polymers and Plastics
- Metals and Alloys