TY - JOUR
T1 - Structure of 6β-acetoxyprogesterone, C23H32O4
AU - Gałdecki, Zdzisław
AU - Grochulski, Paweł
AU - Wawrzak, Zdzisław
AU - Duax, William L.
PY - 1989/12
Y1 - 1989/12
N2 - The X-ray crystal structure of 6 β-acetoxyprogesterone, C23H32O4, has been determined. This compound crystallizes in space group P212121 with a=13.195(3), b=15.035(4), c=10.705(3) Å, V=2139.8(9) Å3, Mr=372.5, Z=4, Dx=1.156g cm-3; Mo Kα radiation (λ=0.7107 Å), μ=0.72 cm-1, F(000)=808;R=0.069, and Rw=0.052 for 1292 reflections. Ring A adopts a normal 1 α,2 β-half-chair conformation. The side chain is typical for a 20-ketosteroid conformation.
AB - The X-ray crystal structure of 6 β-acetoxyprogesterone, C23H32O4, has been determined. This compound crystallizes in space group P212121 with a=13.195(3), b=15.035(4), c=10.705(3) Å, V=2139.8(9) Å3, Mr=372.5, Z=4, Dx=1.156g cm-3; Mo Kα radiation (λ=0.7107 Å), μ=0.72 cm-1, F(000)=808;R=0.069, and Rw=0.052 for 1292 reflections. Ring A adopts a normal 1 α,2 β-half-chair conformation. The side chain is typical for a 20-ketosteroid conformation.
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U2 - 10.1007/BF01160877
DO - 10.1007/BF01160877
M3 - Article
AN - SCOPUS:18544385682
SN - 0277-8068
VL - 19
SP - 949
EP - 955
JO - Journal of Crystallographic and Spectroscopic Research
JF - Journal of Crystallographic and Spectroscopic Research
IS - 6
ER -