Ultrahigh-vacuum furnace for sintering studies of ultrafine ceramic particles

John E. Bonevich*, Mao Hua Teng, D. Lynn Johnson, Laurence Marks

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

2 Scopus citations

Abstract

An ultrahigh-vacuum (UHV) furnace has been designed and constructed for the purpose of investigating the sintering behavior of ultrafine ceramic particles. The UHV furnace has three main chambers for particle production, sintering, and collection with additional facilities for an UHV transfer system. The furnace system achieves a base pressure of 4 × 10-7 Pa through the use of turbomolecular and ion pumps. The ultrafine particles of aluminum oxide are produced by the arc discharge method resulting in the formation of highly faceted particles in the size range of 20-50 nm. The particles are then carried into the tube furnace by a flowing gas stream where they sinter at elevated temperatures. The sintered samples are collected onto a specimen cartridge which is then transported under vacuum conditions to an UHV high-resolution electron microscope for structural characterization. The unique feature of this UHV furnace system is that one is able to perform sintering studies in a clean environment thereby minimizing the influence of contaminating species on the sintering behavior.

Original languageEnglish (US)
Pages (from-to)3061-3067
Number of pages7
JournalReview of Scientific Instruments
Volume62
Issue number12
DOIs
StatePublished - Dec 1 1991

ASJC Scopus subject areas

  • Instrumentation
  • Physics and Astronomy (miscellaneous)

Fingerprint Dive into the research topics of 'Ultrahigh-vacuum furnace for sintering studies of ultrafine ceramic particles'. Together they form a unique fingerprint.

Cite this