TY - JOUR
T1 - (Z)-α-5-Bromo-N-tert-butyl-2-methoxy-phenylnitrone
AU - Guo, Hao
AU - Zabawa, Mark
AU - Woo, Joyce
AU - Zheng, Chong
AU - Yao, Qingwei
PY - 2007
Y1 - 2007
N2 - The title compound, C12H16BrNO2, was synthesized in 95% yield by condensation of 5-bromo-2-methoxy-benzaldehyde and N-tert-butyl-hydroxy-lamine acetate in the presence of triethyl-amine as the base and anhydrous magnesium sulfate as the dehydrating agent. The C=N bond leads to a plane containing all atoms of the side chain, excluding the three methyl groups; this plane makes a dihedral angle of 14.44 (3)° with the ring plane.
AB - The title compound, C12H16BrNO2, was synthesized in 95% yield by condensation of 5-bromo-2-methoxy-benzaldehyde and N-tert-butyl-hydroxy-lamine acetate in the presence of triethyl-amine as the base and anhydrous magnesium sulfate as the dehydrating agent. The C=N bond leads to a plane containing all atoms of the side chain, excluding the three methyl groups; this plane makes a dihedral angle of 14.44 (3)° with the ring plane.
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U2 - 10.1107/S1600536807035568
DO - 10.1107/S1600536807035568
M3 - Article
AN - SCOPUS:35148822810
SN - 1600-5368
VL - 63
SP - o3943
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 10
ER -