(Z)-α-5-Bromo-N-tert-butyl-2-methoxy-phenylnitrone

Hao Guo*, Mark Zabawa, Joyce Woo, Chong Zheng, Qingwei Yao

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

Abstract

The title compound, C12H16BrNO2, was synthesized in 95% yield by condensation of 5-bromo-2-methoxy-benzaldehyde and N-tert-butyl-hydroxy-lamine acetate in the presence of triethyl-amine as the base and anhydrous magnesium sulfate as the dehydrating agent. The C=N bond leads to a plane containing all atoms of the side chain, excluding the three methyl groups; this plane makes a dihedral angle of 14.44 (3)° with the ring plane.

Original languageEnglish (US)
Pages (from-to)o3943
JournalActa Crystallographica Section E: Structure Reports Online
Volume63
Issue number10
DOIs
StatePublished - 2007

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)
  • Condensed Matter Physics

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